There are several avenues for investigation.
1.If you have some untreated parts made in the same batch you can cross section them to determine many things about the heat treat.
2. Cross section a treated piece to determine if there are problems with the metal or with the heat treat.
3. Etch a part to determine if there is grinding burn.
4. Did you do a hardness test before and after?
5. Can you determine if there was a size change in the part during cryogenic processing?
6. Examine worn parts, (treated and untreated) to determine if there is a difference in the wear pattern.
7. Examine your cryoprocessor for problems. Most units out there use a spray bar to cool the parts. If Liquid Nitrogen sprays on to a relatively warm part, it can crack it, especially if it is a very hard M2. I know the people who make these machines will tell you that the nitrogen evaporates before it hits the part, but we have found this to be untrue.
8. What temperature did you temper at,for how long, and how big was the part and how tightly packed in the tempering oven?
9. How many times did yout temper?
10. What cryogenic cycle did you run?