In the plant I worked in, deriming was done with hot N2 gas from stage 2 discharge of the export N2 gas compressors (upstream of aftercooler). I would imagine all air separation plants would have facilities installed for deriming / defrosting of the main ASU cold box with operating instructions. Have you lost the operating manual ? Make sure you have drained out all liquids from the column and that the column has warmed up somewhat , and also keep within the warm up rates prescribed in the Operating manual (degC/hr).