Hello miketech
First, let's slow down a bit and get some more info. Based on your first post, you are not near "bomb" state yet.
1. This unit has an on-load tap changer, but it has only been operated while the unit was out of service?
2. Is the TC a free breather, or sealed and under nitrogen?
3. Is this transformer loaded beyond its nameplate rating on a regular basis, only occasionally, or almost never?
4. If you did a dga prior to the tightening of bolts and filtering, what were the original amounts in ppm of the following?
a. Hydrogen
b. Oxygen
c. Nitrogen
d. Methane (CH4)
e. Ethane (C2H6)
f. Ethylene (C2H4)
g. Acetylene (C2H2)
An acid number would also be very helpful in determining the overall oil condition before your work began. Was there any sludge buildup in the TC or any particulate?
Describe the color of the oil in your sample prior to your filtering and other work.
Please also state whether you simply filtered the oil,(with cartridge type filters in a typical press) or did you process with heat and degas?
Keeping in mind I'm referring to tap changers here, the presence of Ethelene in large amounts in insulating oil is indicative of over heating of components in the tap changer compartment without any arcing. There are several areas where this heating could originate from. Obviously, bolted conections would be a great place to start. However, don't overlook "contact fingers" or other contact areas which rely on spring tension to maintain contact. The compartment should be evacuated, flushed to remove any particulate that may have accumulated, and a very comprehensive inspection made of every single current carrying part of the tap changer. Elevated levels of ethylene can come about by surprisingly small over heated areas or "hot spots". Don't just look at leads, look at everything with a very critical eye. Use bright lights and inspection mirrors to look at ALL parts of the tap changer.