4. Hot bending
(a) The problem
As previously mentioned P91 depends on a specific microstructure for its elevated creep strength properties. Any thermal process such as inter-critical heat treatment or tempering that changes the microstructure could substantially reduce the creep strength so that it approaches, in the worst case, that of 2 ¼%Cr, 1%Mo.
(Note: Inter-critical heat treatment is heating of the material into the temperature range where the microstructure begins to transform from ferrite to austenite. During heating, this process of transformations starts at the lower critical temperature and is completed by the upper critical temperature.)
(b) The solution
Recommendations are before the Code committees to ensure that if it is necessary to normalise and temper P91 material then this process is carried out in the most appropriate temperature ranges.
The temperature ranges recommended for normalising and tempering are 1040-1080°C and 730-800°C respectively.
There is a recommendation in the ASME paper that if any pipe component is heated “locally” above 800°C then the component should be re-normalised and tempered in a manner that will eliminate the zones that have been heated into the inter-critical range.
(c) Other issues
ASME B31.1, clause 129.3.1 requires that hot bending/forming should be carried out at a temperature above the lower critical temperature minus 56°C, i.e. approximately 754°C.
The ASME paper says that significant reductions in creep strength can occur if P91 is exposed to temperatures of the lower critical temperature minus 28°C, i.e. approximately 782°C.
Therefore, to comply with B31.1 and prevent reductions in creep strength while avoiding the need to re-normalise and temper means hot bending should be carried out in the temperature ranges 754-782°C. If this temperature range were selected for hot bending then practical difficulties are expected in maintaining the material temperatures within this range. There is the complication that the lower critical temperature is dependent upon material composition which will vary from batch to batch.
It is understood that hot bending is usually carried in the range 750-950°C.
B31.1, clause 129.3.3(A) states only that any post-hot bending/forming heat treatment should be specified by the designer. There have been cases in the USA when bends that were formed at 1090°C have not been re-normalised and tempered.
If view of the above, we should require all hot bends should be re-normalised and tempered and that the necessary records should be provided to confirm that this has been carried out. This agrees with the requirements stated in the T91/P91 Book.
In the case of ??? project, we should request details of hot bending procedures together with details of any subsequent heat treatment.