dgillete, it is not a violation. It can as the material changes phases. It is all due to the pressure increases from the normal and shear stresses, and temperature fluctuations in the lab. This is a little known secret since the material changes back to the original state after the pressure is removed and the samples are observed.
On another note:
Items to think about:
1. You have run a test that will have only a certain amount of precision (as in the actual numbers could be +- the number you obtained).
2. You only have two data points, and are basing your decisions off of them. Often a third point is done and a best fit line is drawn.
3. You have extrapolated the result back to zero, and this negative result is not based on an actual data point.
4. There is potential that there is a nonlinear strength envelope, even though we normally make it so.
5. The result is only below zero by 18psf, and it is not like it is 500psf.
6. Perhaps some engineering judgment should be applied. Test results are meaningless without it.