STYMIEDPIPER:
We actually do the testing as part of our services, both in the shop and in the field.
We use both Vacuum and Pressure type testing, depending on the application. Each application has its positive and negative sides.
For existing acid piping we would most likely use the pressure method. Based on the parameters of the system we would pressurize with either pure Helium or a Helium/Nitrogen mixture (to control costs for larger volumes). The test pressure needs to be only a few PSI, but the higher you can go the easier and quicker it is to get the results. Also, using the pressure method you do not need to clean out the piping system in order to do the test. The Helium will find its way through thin films of residue and then through the leak path. It really is a powerful tool. The testing can be performed without dismantling the system which saves a great deal of time and money. All you need to do to be able to test is isolate the piping and have a port to supply the tracer gas. Most systems have these requirements in place already.
BigInch:
There is no practical physical limit for the equipment being tested, but an engineering evaluation needs to be performed prior to the start of any testing to ensure the equipment is able to withstand the test process. For high volumes like you describe we would mix the Helium with another inert gas such as Nitrogen to about 5% Helium and still be able to get meaningful results. If your pipeline in new or in clean service, it may be more advantageous to examine the vacuum process where the amount of Helium used is very small. The trick with this method is to ensure that the system can handle the vacuum condition without collapsing. An evaluation of the project at the outset will determine the best approach.