mks07;
Have you followed the advice of weldstan above? If you have already removed the sample without involvement of the lab metallurgist, the following minimum steps would be recommended;
1. Macrophotos of the sample showing the orientation and location of the crack(s). Orientation of the sample relative to the pressure vessel is critical and must be identified and marked on the sample at the time of removal. Surface NDE might be required to highlight cracks.
2. Dimensions of the sample and observed crack lengths.
3. Careful extraction of one or more cracks to expose (break open) the fracture surface for examination.
4. SEM of the fracture surfaces - option.
5. Depending on the results of step 4, prepare one or more samples containing a cross section of the fracture surface for metallographic examination. Compare with sample removed and prepared for metallographic examination away from the fracture surface.
6. Complete chemical analysis of the sample material.
7. Perform hardness testing to evaluate hardness through thickness.
The above are recommended with other steps added depending on the results.